Synthesis, Mechanical Properties and Thermal Stability Of Polydimethylsiloxane Nanocomposites

Jump To References Section

Authors

  • Department of Sciences and Humanities, School of Engineering and Technology, CHRIST (Deemed to be University), Bengalure - 560074, Karnataka ,IN
  • Department of Sciences and Humanities, School of Engineering and Technology, CHRIST (Deemed to be University), Bengalure - 560074, Karnataka ,IN

DOI:

https://doi.org/10.18311/jmmf/2023/36262

Keywords:

Mechanical Properties, Nanocomposites, Nano-graphite, Polydimethylsiloxane, Thermal Properties

Abstract

The polydimethylsiloxane/nano-graphite (PDMS-NG) nanocomposites were prepared via a two rolled mixing mill and subjected to characterization using techniques such as Transmission Electron Microscopy (TEM), stress-strain analysis during elongation, as well as thermal properties including Thermo-Gravimetric Analysis (TGA) and Differential Scanning Calorimetry (DSC). The transition temperature was observed to be below -70°C for PDMS nanocomposites reinforced with Nano-Graphite (NG). The thermogram from the thermo-gravimetric analysis indicated that at 10%, 20%, 30%, and 50% weight loss, the temperatures for PDMS nanocomposites were higher compared to unfilled PDMS. These findings suggest a substantial improvement in the thermal stability of PDMS-NG nanocomposites.

Downloads

Download data is not yet available.

Metrics

Metrics Loading ...

Downloads

Published

2023-11-30

How to Cite

Saji, J., & Money, B. K. (2023). Synthesis, Mechanical Properties and Thermal Stability Of Polydimethylsiloxane Nanocomposites. Journal of Mines, Metals and Fuels, 71(11), 1971–1978. https://doi.org/10.18311/jmmf/2023/36262

 

References

Park HH, Jana SC. The relationship between nano- and micro-structures and mechanical properties in PMMA–epoxy–nanoclay composites. Polymer. 2003; 44:2091-2100. DOI: https://doi.org/10.1016/S0032-3861(03)00075-2

Usuki A, Kojima Y, Kawasumi M, Okada A, Fukushim Y, Kurauchi T, Kamigaito O. Synthesis of nylon 6-clay hybrid. Journal of Materials Research. 1993; 8:1179- 1184. DOI: https://doi.org/10.1557/JMR.1993.1179

Alexandre M, Dubois P. Polymer-layered silicate nano- composites: preparation, properties and uses of a new class of materials. Material Science and Engineering. 2000; 28:1-63. DOI: https://doi.org/10.1016/S0927-796X(00)00012-7

Mousa A, Karger-Kocsis. Rheological and ther- modynamical behavior of styrene/butadiene rubber-organoclay nanocomposites. Macromolecular Materials and Engineering. 2001; 286:260-266. DOI: https://doi.org/10.1002/1439-2054(20010401)286:4<260::AID-MAME260>3.3.CO;2-O

Sur GS, Sun HL, Lye SG, Mark JE. Synthesis, structure, mechanical properties, and thermal stability of some polysulfone/organoclay nanocomposites. Polymer. 2001; 42:9783-9789. DOI: https://doi.org/10.1016/S0032-3861(01)00527-4

Turi EA. Thermal characterization of polymeric materi- als. 2nd edn., Academic Press, New York, 1997.

Maurer JJ, Brazier DW. Applications of thermal analysis in the rubber industry. Kautschuk.Gummi Kunststoffe. 1983; 36:37-45.

Sircar AK. Analysis of elastomer vulcanizate composi- tion by TG-DTG Techniques. Rubber Chemistry and Technology. 1992; 65(3):503-526. DOI: https://doi.org/10.5254/1.3538627

Sircar AK, Lamond TG. Identification of elastomers by thermal analysis. Rubber Chem Technol. 1972; 45(1):329-345. DOI: https://doi.org/10.5254/1.3544710

Dutta NK, Tripathy DK. Effects of types of fillers on the molecular relaxation characteristics, dynamic mechani- cal, and physical properties of rubber vulcanizates. J Appl Polym Sci. 1992; 44:1635-1648. DOI: https://doi.org/10.1002/app.1992.070440918

Choudhury NR, Bhowmick AK. Thermal char- acterization of thermoplastic elastomeric natural rubber-polypropylene blends. Thermochimica Acta. 1991; 176:149-161. DOI: https://doi.org/10.1016/0040-6031(91)80270-S

Saji J. Thermal Studies of Multiwalled Carbon Nanotube Reinforced with Silicone Elastomer Nanocomposites. Materials Today: Proceedings. 2019; 11:935–943. DOI: https://doi.org/10.1016/j.matpr.2018.12.022